Ruthenium (II) complexes of NO ligands: Synthesis, characterization and application in transfer hydrogenation of carbonyl compounds
Journal of Organometallic Chemistry, ISSN: 0022-328X, Vol: 801, Page: 122-129
2016
- 38Citations
- 36Captures
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Article Description
New Schiff base ligands including azo group such as (4-((E)-(4-ethylphenyl)diazenyl)-2-((E)-(phenylimino)methyl)phenol 2, 4-((E)-(4-ethylphenyl)diazenyl)-2-((E)-(naphthalen-1-ylimino)methyl)phenol 3, 2-((E)-(benzylimino)methyl)-4-((E)-(4-ethylphenyl)diazenyl)phenol 4 and azo group-free ligand (E)-2-((benzylimino)methyl)phenol 8 and their ruthenium complexes 5 – 7 and 9 with [RuCl 2 ( p -cymene)] were synthesized and characterized by spectroscopic techniques including 1 H and 13 C NMR, FT-IR and UV–Vis. According to the UV–visible, IR and NMR data, the Ru (II) complexes 5–7 and 9 are formed by the coordination of N, O atoms of the ligands. Molecular structures of the complex 7 and complex 9 were determined by single crystal X-ray diffraction studies. These Ruthenium (II) complexes 5–7 and 9 were used as catalysts for the transfer hydrogenation of a series of ketones and benzaldehyde in 2-propanol. Following the comparison of complex 9 with the other three azo containing complexes 5–7, it was observed that azo group has got remarkable increasing effect on the catalytic activity. The results showed that the complex 5 is efficient than the other Ru (II) complexes.
Bibliographic Details
http://www.sciencedirect.com/science/article/pii/S0022328X15301996; http://dx.doi.org/10.1016/j.jorganchem.2015.10.028; http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=84946748928&origin=inward; https://linkinghub.elsevier.com/retrieve/pii/S0022328X15301996; https://dx.doi.org/10.1016/j.jorganchem.2015.10.028
Elsevier BV
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