Synthesis and characterization of the "sulfur-rich" bis(perthiobenzoato)(dithiobenzoato)technetium(III) heterocomplex
Inorganic Chemistry, ISSN: 0020-1669, Vol: 41, Issue: 3, Page: 598-601
2002
- 40Citations
- 6Captures
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Metrics Details
- Citations40
- Citation Indexes40
- 40
- CrossRef32
- Captures6
- Readers6
Article Description
Formation of the mixed bis(perthiobenzoato)dithiobenzoato - Tc(III) heterocomplex [Tc(SCPh)(SCPh)] (1) is achieved via reduction-substitution reactions of excess dithiobenzoate piperidinium salt with labile high-valent [Tc(O)Cl] or [Tc(N)Cl] precursors. Partial oxidation of the ligand affords a coordination sphere that is totally filled by sulfur donor atoms of different nature. Hence, the combination of π-donor and π-acceptor sulfurs produces a peculiar distorted octahedral environment characterized by the substitution-inert metal fragment [Tc(SCPh)] and the substitution-labile dithiobenzoato coligand.
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