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Tridentate complexes of 2,6-bis(4-substituted-1,2,3-triazol-1-ylmethyl) pyridine and its organic azide precursors: An application of the copper(II) acetate-accelerated azide-alkyne cycloaddition

Dalton Transactions, ISSN: 1477-9226, Vol: 40, Issue: 14, Page: 3655-3665
2011
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Rapid coupling reactions between 2,6-bis(azidomethyl)pyridine and terminal alkynes in the presence of 5 mol% Cu(OAc)·HO without the addition of a reducing agent afford tridentate ligands for first-row transition-metal ions. The chelation between Cu and alkylated nitrogen atoms of the azido groups of 2,6-bis(azidomethyl)pyridine, as observed in the solid state, is credited for the acceleration of the azide-alkyne cycloaddition reactions. © The Royal Society of Chemistry 2011.

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