Semi-real-time pure shift NMR spectroscopy

Publication Year:
2018

No metrics available.

DOI:
10.17632/wc57dfv6zs.1
Author(s):
Morris, Gareth
Publisher(s):
Mendeley
Tags:
Nuclear Magnetic Resonance Spectroscopy
data summary

Pulse sequence code, macros, and example data for 1D band-selective semi-real-time pure shift NMR experiments Peter Kiraly, Mathias Nilsson, Gareth A. Morris NMR Methodology Group University of Manchester Nov 2017 ============================================================================================================= Experimental data [\data] \data\Fig-3 Sample details: 5mM cyclosporine in CD2Cl2 a.fid conventional proton experiment b.fid time-shared homodecoupling c/d/e/f_raw-data.fid raw data of interferogram/real time/WATERGATE-semi-real-time/semi-real-time experiments c/d/e/f_proc-data.fid processed data of interferogram/real time/WATERGATE-semi-real-time/semi-real-time experiments \data\Fig-4 Sample details: 0.05mM cyclosporine in CD2Cl2 a.fid conventional proton experiment b.fid time-shared homodecoupling c/d/e/f_raw-data.fid raw data of interferogram/real time/WATERGATE-semi-real-time/semi-real-time experiments c/d/e/f_proc-data.fid processed data of interferogram/real time/WATERGATE-semi-real-time/semi-real-time experiments Left and Right in filenames refers to the selected NH and CH region \data\Fig-5 Sample details: 0.58M 2,3-dibromothiophene in dmso-d6 (doped with chromium-acetylacetonate) a.fid conventional proton experiment b.fid time-shared homodecoupling without BS compensation c.fid time-shared homodecoupling with BS compensation d/e/f/g_raw-data.fid raw data of interferogram/real time/WATERGATE-semi-real-time/semi-real-time experiments d/e/f/g_proc-data.fid processed data of interferogram/real time/WATERGATE-semi-real-time/semi-real-time experiments \data\Fig-6 Sample details: 5mM cyclosporine in CD2Cl2 a.fid time-shared homodecoupling b.fid 1D band-selective TOCSY c.fid 1D sleective DQF-COSY d.fid conventional proton \data\Fig-7 Sample details: 2.5mM mixture of R/S-ibuprofen and 10mM beta-cyclodextrin in D2O a.fid conventional proton experiment b.fid time-shared homodecoupling using 10Hz SEDUCE-2 c.fid time-shared homodecoupling using 25Hz DSNOB d/e/f/g_raw-data.fid raw data of interferogram/real time/WATERGATE-semi-real-time/semi-real-time experiments d/e/f/g_proc-data.fid processed data of interferogram/real time/WATERGATE-semi-real-time/semi-real-time experiments ============================================================================================================= Macro files [\maclib] go_kp_ifPSZS_1d_01 go_kp_rtPSZS_1d_02 go_kp_srtPSZS_1d_02 kp_ifZSproc2 kp_makePS7 kp_makePS9 kp_rtACQ31_proc_v3 kp_srtACQ31_proc_v6 ============================================================================================================= Pulse sequence files [\psglib] kp_ifPSZS_1d_01.c kp_rtPSZS_1d_02.c kp_srtPSZS_1d_02.c =============================================================================================================