The microwave spectrum, structure and dipole moment of cyclobutene ozonide (2,3,7-trioxabicyclo[2.2.1]heptane)
Journal of Molecular Structure, ISSN: 0022-2860, Vol: 190, Issue: C, Page: 125-133
1988
- 16Citations
- 1Usage
- 2Captures
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Metrics Details
- Citations16
- Citation Indexes16
- CrossRef16
- Usage1
- Abstract Views1
- Captures2
- Readers2
Article Description
Cyclobutene ozonide containing deuterium, 13 C and 18 O enrichment was prepared by ozonolysis of cyclobutene and via singlet molecular oxygen addition to furan. It was established that the ozonide has C s symmetry. The structure was determined from the assignment of the microwave spectra of eight isotopic species. The peroxy bond distance of 1.492(5) Å is increased by about 0.03 Å compared with less strained monocyclic ozonides. The ring strain is also evident in several other bond distances and angles when compared with cyclopentene ozonide. The dipole moment is 2.857(2) debye.
Bibliographic Details
http://www.sciencedirect.com/science/article/pii/0022286088802771; http://dx.doi.org/10.1016/0022-2860(88)80277-1; http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=0001764875&origin=inward; https://linkinghub.elsevier.com/retrieve/pii/0022286088802771; https://api.elsevier.com/content/article/PII:0022286088802771?httpAccept=text/xml; https://api.elsevier.com/content/article/PII:0022286088802771?httpAccept=text/plain; https://digitalcommons.mtu.edu/michigantech-p/5353; https://digitalcommons.mtu.edu/cgi/viewcontent.cgi?article=24655&context=michigantech-p; http://dx.doi.org/10.1016/0022-2860%2888%2980277-1; https://dx.doi.org/10.1016/0022-2860%2888%2980277-1
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