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Diastereoselective [3 + 2] Cycloaddition between Tertiary Amine N-Oxides and Substituted Alkenes to Access 7-Azanorbornanes

Organic Letters, ISSN: 1523-7052, Vol: 26, Issue: 31, Page: 6546-6550
2024
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Article Description

We have developed a diastereoselective synthesis of 43 novel 7-azanorbornanes using tertiary amine N-oxides and substituted alkenes. Our method uses an efficient [3 + 2] cycloaddition, starting from either commercially available or easily accessible precursors to generate yields up to 97% and diastereomeric ratios up to >20:1. Density functional theory (DFT) calculations were performed, suggesting that the observed diastereoselectivity is likely due to steric considerations.

Bibliographic Details

Alexander H. Cocolas; Aiden M. Lane; Benjamin S. Musiak; Eric J. Chartier; Derek A. Bedillion; Sarah L. Hejnosz; Paul A. Lummis; Jeffrey D. Evanseck; Thomas D. Montgomery; Jeffrey J. Rohde

American Chemical Society (ACS)

Biochemistry, Genetics and Molecular Biology; Chemistry

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