Preparation and Characterization of some Polyalkylarylamines.(Dept.P)
MEJ. Mansoura Engineering Journal, Vol: 13, Issue: 2, Page: 27-37
2021
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Article Description
Adducts of polyalkylarylamines will stoichiometric amounts of stannous chloride were obtained by the reaction of 1,2-dichloroethane with m-phenylenediamine, p-phenylenediamine and 4,4 diaminodiphenyl in the presence of hydrochloric acid and stoichiometric amounts of stannous chloride in methanol as a solvent. Also, adduct of poly (chloromethyne-co- 4,4-dianiinodiphenyl) was obtained from the reaction of chloroform and benzidine by similar method. The structure of these adducts was confirmed by JR spectroscopy, as well 0.X-ray diffractometery, These adducts when reacted with aqueous solution of ammonium carbonate gave the corresponding polyalkylaryl-amine hydrochlorides. Also thermal analysis of these adducts were carried out .
Bibliographic Details
Egypts Presidential Specialized Council for Education and Scientific Research
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