Model epoxy/metal-oxide chemical interactions: diethanolamine on oxidized copper and aluminum
Applied Surface Science, ISSN: 0169-4332, Vol: 59, Issue: 3, Page: 273-280
1992
- 24Citations
- 1Usage
- 8Captures
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Metrics Details
- Citations24
- Citation Indexes24
- 24
- CrossRef19
- Usage1
- Abstract Views1
- Captures8
- Readers8
Article Description
Diethanolamine (DEA), a model compound for an amine cured epoxy resin, was absorbed from dilute ethanol solutions onto air-oxidized Cu, air-oxidized Al and phosphoric acid-anodized Al. The adsorbate/substrate chemical interactions were probed by X-ray photoelectron spectroscopy (XPS). XPS monitoring of DEA coverage on air-oxidized Al as a function of temperature in ultrahigh vacuum shows that significant thermal desorption begins only above 500 K, demonstrating that specific chemical bonding interactions do occur between an amine-cured epoxy and a “real world” oxide surface. DEA desorption temperatures and N ls binding energies are consistent with N tone-pair coordination to acidic aluminum sites.
Bibliographic Details
http://www.sciencedirect.com/science/article/pii/016943329290128K; http://dx.doi.org/10.1016/0169-4332(92)90128-k; http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=0026897037&origin=inward; http://linkinghub.elsevier.com/retrieve/pii/016943329290128K; http://api.elsevier.com/content/article/PII:016943329290128K?httpAccept=text/xml; http://api.elsevier.com/content/article/PII:016943329290128K?httpAccept=text/plain; https://linkinghub.elsevier.com/retrieve/pii/016943329290128K; https://api.elsevier.com/content/article/PII:016943329290128K?httpAccept=text/xml; https://api.elsevier.com/content/article/PII:016943329290128K?httpAccept=text/plain; https://scholarsmine.mst.edu/matsci_eng_facwork/1079; https://scholarsmine.mst.edu/cgi/viewcontent.cgi?article=2078&context=matsci_eng_facwork; http://dx.doi.org/10.1016/0169-4332%2892%2990128-k; https://dx.doi.org/10.1016/0169-4332%2892%2990128-k
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