Determination of nickel in soy milk powder by ultra-wave digestion-inductively coupled plasma mass spectrometry
Vol: 38, Issue: 3, Page: 60-64
2022
- 30Usage
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Example: if you select the 1-year option for an article published in 2019 and a metric category shows 90%, that means that the article or review is performing better than 90% of the other articles/reviews published in that journal in 2019. If you select the 3-year option for the same article published in 2019 and the metric category shows 90%, that means that the article or review is performing better than 90% of the other articles/reviews published in that journal in 2019, 2018 and 2017.
Citation Benchmarking is provided by Scopus and SciVal and is different from the metrics context provided by PlumX Metrics.
Metrics Details
- Usage30
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- Abstract Views8
Artifact Description
Objective:This study aimed to provides technical support for the risk prevention and control of nickel contamination in market soy milk powder.Methods:With concentrated nitric acid as digestion solution, the ultra-wave digestion was utilized for preprocessing, and then the ICP-MS, with Rhodium as internal standard to eliminate matrix interference and in the KED mode, was used to determine the content of nickel in soybean milk powder. Moreover, the conditions for ultra-wave digestion and ICP-MS were also optimized.Results:The linear relationship of the standard curves was located within the mass concentration of 0~10 μg/L, with correlation coefficient of 0.999 9, and the detection limit was 0.002 mg/kg. The recovery percent ranged form 94.5% to 100.6% and the relative standard deviation (RSD)was 1.8%~2.3%. The proposed method was validated on the quality control sample of soy milk powder (ZKQC5210) and the determination result was in the certification scope.Conclusion:The proposed method was correct and reliable, so it was suitable for the determination of the nickel content in soybean milk powder.
Bibliographic Details
https://www.ifoodmm.cn/journal/vol38/iss3/9; https://www.ifoodmm.cn/cgi/viewcontent.cgi?article=1084&context=journal; http://dx.doi.org/10.13652/j.spjx.1003.5788.2022.90062; https://dx.doi.org/10.13652/j.spjx.1003.5788.2022.90062; https://www.chndoi.org/Resolution/Handler?doi=10.13652/j.spjx.1003.5788.2022.90062
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