Nickel-Catalyzed Reductive Coupling of Carboxylic Acids with Disulfides to Access Thioesters
Advanced Synthesis and Catalysis, ISSN: 1615-4169, Vol: 365, Issue: 23, Page: 4233-4240
2023
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Article Description
A nickel-catalyzed reductive cross coupling reaction of carboxylic acids with disulfides is described. The readily available and inexpensive carboxylic acid is activated in situ by the formation of a mixed anhydride. The transformation occurs at room temperature with wide functional group tolerance to efficiently generate structurally diverse thioesters. Moreover, the reaction tolerated a broad substrate scope, including sterically hindered of disulfides. Ultimately, this powerful method could be applied to the late-stage functionalization for the construction of diverse thioesters, affording a convenient and practical tactic to construct carbon-sulfur bonds.
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