Automated headspace solid-phase microextraction and on-fiber derivatization for the determination of clenbuterol in meat products by gas chromatography coupled to mass spectrometry
Journal of Separation Science, ISSN: 1615-9314, Vol: 38, Issue: 3, Page: 418-425
2015
- 20Citations
- 27Captures
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Example: if you select the 1-year option for an article published in 2019 and a metric category shows 90%, that means that the article or review is performing better than 90% of the other articles/reviews published in that journal in 2019. If you select the 3-year option for the same article published in 2019 and the metric category shows 90%, that means that the article or review is performing better than 90% of the other articles/reviews published in that journal in 2019, 2018 and 2017.
Citation Benchmarking is provided by Scopus and SciVal and is different from the metrics context provided by PlumX Metrics.
Metrics Details
- Citations20
- Citation Indexes20
- 20
- CrossRef15
- Captures27
- Readers27
- 27
Article Description
A method was developed for the determination of clenbuterol in meat using stable-isotopedilution gas chromatography with mass spectrometry coupled with solid-phase microextraction and on-fiber derivatization. The samples were first homogenized with hydrochloric acid followed by protein deposition. After headspace solid-phase microextraction and onfiber derivatization, the content of clenbuterol was measured with the aid of stable-isotope dilution. The condition of solid-phase microextraction was optimized by central composite design. The relative standard deviations, limit of detection, and recoveries for clenbuterol were 4.2-9.2%, 0.48 g/kg, and 96-104%, respectively. The proposed method was satisfactory for analysis of real samples as compared with the Chinese standard method.
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=84923007698&origin=inward; http://dx.doi.org/10.1002/jssc.201400634; http://www.ncbi.nlm.nih.gov/pubmed/25403577; https://onlinelibrary.wiley.com/doi/10.1002/jssc.201400634; https://dx.doi.org/10.1002/jssc.201400634; https://analyticalsciencejournals.onlinelibrary.wiley.com/doi/10.1002/jssc.201400634
Wiley
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