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Complete H and C NMR assignments of clerodane diterpenoids of Salvia splendens

Magnetic Resonance in Chemistry, ISSN: 1097-458X, Vol: 44, Issue: 10, Page: 962-965
2006
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Article Description

Unambiguous and complete assignments of H and C NMR chemical shifts for five clerodane diterpenes, four of them isolated from Salvia splendens (salviarin, splendidin and splenolides A and B) and one obtained by acetylation of splenolide A, are presented. The assignments are based on 2D shift-correlated [H,H-COSY, H,C-gHSQC-J(C,H) and H, C-gHMBC-J(C,H) (n = 2 and 3)] and nuclear Overhauser effect (NOE) experiments. The conformation of the rings of these compounds is supported by the J(H,H) values and NOE results. Copyright © 2006 John Wiley & Sons, Ltd.

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