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Ruthenium(III) chloride-catalyzed efficient protocol for ethyl diazoacetate insertion into the N-H bond of secondary amines

Monatshefte fur Chemie, ISSN: 0026-9247, Vol: 139, Issue: 11, Page: 1369-1372
2008
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Ruthenium(III) chloride (1 mol%) alone can catalyze the insertion of ethyl diazoacetate into N-H bonds of various structurally and electronically diverse secondary cyclic amines under solvent-free conditions to afford the corresponding glycine esters in good yields under ambient conditions. Reactions with various aliphatic primary and aromatic amines examined, however, were unsuccessful. © 2008 Springer-Verlag.

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