Enantioseparation of the new antifungal drug iodiconazole and structurally related triadimenol analogues by CE with neutral cyclodextrin additives
Chromatographia, ISSN: 0009-5893, Vol: 73, Issue: 9-10, Page: 1009-1014
2011
- 16Citations
- 9Captures
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Article Description
Chiral separation of iodiconazole, a new antifungal drug, and 12 new structurally related triadimenol analogues were studied by capillary electrophoresis with seven neutral cyclodextrins. It was found that hydroxypropyl-γ-cyclodextrin (HP-γ-CD) was the most effective chiral selector. Furthermore, the influence of the concentration of HP-γ-CD, buffer pH, buffer concentration, temperature, and applied voltage was investigated, and the method was validated. The study of the analyte structure-enantioseparation relationships showed that substitutions in the side chains had important influences on enantiomeric separation. © Springer-Verlag 2011.
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=79958286673&origin=inward; http://dx.doi.org/10.1007/s10337-010-1897-y; http://link.springer.com/10.1007/s10337-010-1897-y; http://link.springer.com/content/pdf/10.1007/s10337-010-1897-y; http://link.springer.com/content/pdf/10.1007/s10337-010-1897-y.pdf; http://link.springer.com/article/10.1007/s10337-010-1897-y/fulltext.html; https://dx.doi.org/10.1007/s10337-010-1897-y; https://link.springer.com/article/10.1007/s10337-010-1897-y; http://www.springerlink.com/index/10.1007/s10337-010-1897-y; http://www.springerlink.com/index/pdf/10.1007/s10337-010-1897-y
Springer Science and Business Media LLC
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