Investigation of organotin (IV) thiosemicarbazones precursors for synthesizing nanoscaled tin tulfide materials
Journal of Materials Science: Materials in Electronics, ISSN: 1573-482X, Vol: 35, Issue: 6
2024
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Investigators at Manipal University Report Findings in Chemicals and Chemistry [Investigation of Organotin (Iv) Thiosemicarbazones Precursors for Synthesizing Nanoscaled Tin Tulfide Materials]
2024 MAY 09 (NewsRx) -- By a News Reporter-Staff News Editor at Health & Medicine Daily -- Fresh data on Chemicals and Chemistry are presented
Article Description
A sequence of organotin (IV) thiosemicarbazone addition of the type of RSnCl.mLH (1–14) were formed by the reactions of RSnCl with ligands (LH), carvone thiosemicarbazone, CHNS and carvone ethylthiosemicarbazone, CHNS in anhydrous ethanol [where R = CH, CH or CH; n = 2–3 and m = 1–2]. Characterization of all the compounds is done by FT-IR (Fourier-Transform Infrared Spectroscopy), H, C, Sn NMR (Nuclear Magnetic Resonance) and FAB (Fast Atom Bombardment) mass studies. In the solution state, Sn NMR investigations indicate a monodentate method of ligand attachment with the core tin atom through the sulphur atom. TGA(Thermogravimetric Analysis) of (CH)SnCl.2CHNS and (CH)SnCl.2CHNS depicts big thermal events. Transformations of (CH)SnCl.2CHNS and (CH)SnCl.2CHNS to pure tin sulfide (SnS(i) and SnS(ii), correspondingly have been done using solvothermal technique. Images of SEM for (i) and (ii) represents plate-like morphologies of the crystallites and powder XRD(X-Ray Diffraction) of generated tin sulfides suggested formation of orthorhombic structure.
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Springer Science and Business Media LLC
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