Two New {PW} Wheel-shaped Tungstophosphates Decorated by Co(II), Ni(II) Ions
Journal of Cluster Science, ISSN: 1040-7278, Vol: 21, Issue: 4, Page: 679-689
2010
- 20Citations
- 7Captures
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Article Description
Two new wheel-shaped tungstophosphates based on 3d-transition metals (Co(II), Ni(II)) ions decorated [PWO] anion (TM-{PW}), KNa{[Co(HO)Cl][Co(HO)][Co(HO)] [Co(HO)HPWO(HO)]}·2NaCl·41·5HO 1 and Na{[Ni(HO)][{Ni(HO)}HPWO (HO)]}·41. 5HO 2 have been synthesized by routine synthetic reaction of hexavacant Dawson polyoxonanion [PWO] with divalent 3d transition-metal ions in aqueous solution. The two compounds are characterized by elemental analysis, IR spectroscopy, TG analysis, electrochemical analysis, and single-crystal X-ray diffraction. Both compounds contain a 2D layer-like structure constructed from 1D chains of wheel-type [PWO] anions bridged via CoO or NiO units. Cyclic voltammograms and P NMR analysis suggest that the polyanion [PWO] of both compounds are stable in aqueous solution (pH = 4). © 2010 Springer Science+Business Media, LLC.
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=78650226574&origin=inward; http://dx.doi.org/10.1007/s10876-010-0286-x; http://link.springer.com/10.1007/s10876-010-0286-x; http://link.springer.com/content/pdf/10.1007/s10876-010-0286-x; http://link.springer.com/content/pdf/10.1007/s10876-010-0286-x.pdf; http://link.springer.com/article/10.1007/s10876-010-0286-x/fulltext.html; http://www.springerlink.com/index/10.1007/s10876-010-0286-x; http://www.springerlink.com/index/pdf/10.1007/s10876-010-0286-x; https://dx.doi.org/10.1007/s10876-010-0286-x; https://link.springer.com/article/10.1007/s10876-010-0286-x
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