Thermodynamic characteristics of phase conversion of structural isomers for volatile complex of ruthenium (III) trifluoroacetylacetonate
Journal of Thermal Analysis and Calorimetry, ISSN: 1388-6150, Vol: 101, Issue: 1, Page: 41-44
2010
- 11Citations
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Conference Paper Description
The comprehensive analysis of volatile β-diketonate compound-ruthenium(III) trifruoroacetylacetonate (Ru(tfac))-was carried out. By means of flow method in quasi-equilibrium conditions and static method the temperature dependencies of saturated vapor pressure have been measured over solid and liquid cis- and trans-modifications of Ru(tfac) and isomer mixture. The thermodynamic characteristics of sublimation, evaporation, melting, and phase conversion have been calculated for structural isomers. Also by differential-scanning calorimetry the temperature meanings and the thermodynamic characteristics of melting have been determined for individual isomers of Ru(tfac) and their mixtures. By XRD the structures for cis- and trans-modifications have been determined. Both structures consist of neutral molecules arranged in pseudo layers. © 2010 Akadémiai Kiadó, Budapest, Hungary.
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=77954086899&origin=inward; http://dx.doi.org/10.1007/s10973-010-0859-9; http://link.springer.com/10.1007/s10973-010-0859-9; http://link.springer.com/content/pdf/10.1007/s10973-010-0859-9; http://link.springer.com/content/pdf/10.1007/s10973-010-0859-9.pdf; http://link.springer.com/article/10.1007/s10973-010-0859-9/fulltext.html; https://dx.doi.org/10.1007/s10973-010-0859-9; https://link.springer.com/article/10.1007/s10973-010-0859-9; http://www.springerlink.com/index/10.1007/s10973-010-0859-9; http://www.springerlink.com/index/pdf/10.1007/s10973-010-0859-9
Springer Science and Business Media LLC
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