Determination of heat capacities and thermodynamic properties of Al(OH)(OCH)(HN-BDC)
Journal of Thermal Analysis and Calorimetry, ISSN: 1588-2926, Vol: 135, Issue: 6, Page: 3233-3239
2019
- 1Citations
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Metrics Details
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Article Description
The molar heat capacities of one–three-dimensional metal–organic frameworks Al(OH)(OCH)(HN-BDC) (CAU-1) were measured by temperature-modulated differential scanning calorimetry (TMDSC) over the temperature range from 213 to 393 K for the first time. No phase transition or thermal anomaly was observed in the experimental temperature range. The fundamental thermodynamic parameters such as entropy and enthalpy relative to 298.15 K were calculated based on the experimentally determined molar heat capacities. The compound was characterized by elemental analysis, powder XRD, FT-IR spectrum. Moreover, the thermal stabilities and decomposition mechanisms of hydrated phase and dehydrated phase of CAU-1 were investigated by thermogravimetric spectrometer in the temperature range 298–1023 K.
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=85051773900&origin=inward; http://dx.doi.org/10.1007/s10973-018-7608-x; http://link.springer.com/10.1007/s10973-018-7608-x; http://link.springer.com/content/pdf/10.1007/s10973-018-7608-x.pdf; http://link.springer.com/article/10.1007/s10973-018-7608-x/fulltext.html; https://dx.doi.org/10.1007/s10973-018-7608-x; https://link.springer.com/article/10.1007/s10973-018-7608-x
Springer Science and Business Media LLC
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