Synthesis of anisotropic CuS-based nanostructures by thermal oxidation
Journal of Thermal Analysis and Calorimetry, ISSN: 1588-2926, Vol: 138, Issue: 6, Page: 4321-4329
2019
- 12Citations
- 14Captures
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Example: if you select the 1-year option for an article published in 2019 and a metric category shows 90%, that means that the article or review is performing better than 90% of the other articles/reviews published in that journal in 2019. If you select the 3-year option for the same article published in 2019 and the metric category shows 90%, that means that the article or review is performing better than 90% of the other articles/reviews published in that journal in 2019, 2018 and 2017.
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Article Description
Flower-like copper sulfides nanostructures were synthesized via the solvothermal route. The structural, optical and electrochemical properties of the synthesized materials were characterized by means of X-ray diffraction (XRD), scanning electron microscopy, ultraviolet–visible spectrometry and Fourier transform infrared spectroscopy (FTIR). Thermal behavior of the obtained flower-like materials was analyzed by TG, XRD and FTIR in situ measurements, over the temperature range of 25–800 °C. It was found that both shape and phase composition remain stable until the temperature reaches 200 °C. Phase transformation mechanism was discussed. During annealing, mixture of CuS and CuS is converted to copper sulfide hydroxides (200–500 °C) and further to CuO (700 °C and higher). Nevertheless, hierarchically porous structure is stable only to 200 °C. Applying higher temperatures affects the solubility of the material and inflicts structural damage, resulting in the formation of dense oval particles with size of 20 to 200 nm.
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=85070238782&origin=inward; http://dx.doi.org/10.1007/s10973-019-08622-w; http://link.springer.com/10.1007/s10973-019-08622-w; http://link.springer.com/content/pdf/10.1007/s10973-019-08622-w.pdf; http://link.springer.com/article/10.1007/s10973-019-08622-w/fulltext.html; https://dx.doi.org/10.1007/s10973-019-08622-w; https://link.springer.com/article/10.1007/s10973-019-08622-w
Springer Science and Business Media LLC
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