Synthesis, structure and catalytic activity of an oxo-bridged dinuclear oxovanadium complex of an isonicotinohydrazide ligand
Transition Metal Chemistry, ISSN: 0340-4285, Vol: 38, Issue: 3, Page: 267-273
2013
- 25Citations
- 13Captures
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Article Description
A mononuclear dioxo vanadium(V) complex of a hydrazone ONO donor ligand, [VO(L)] (1), was synthesized by the reaction of VO and terephthalic acid with HL in 1:1:1 mol ratio, while an oxo-bridged bis(vanadium(IV)oxo) complex, [μ -O-{VO(L)}] (2), was synthesized by the treatment of isonicotinic acid hydrazide, salicylaldehyde and CoSO·7HO with bis(acetylacetonato)oxovanadium(IV) (HL = isonicotinic acid(2-hydroxy-benzylidene)-hydrazide, HL = isonicotinic acid (1-methyl-3-oxo-butylidene)-hydrazide). The complexes were characterized by elemental analyses and spectroscopic methods. The crystal structure of complex 2 was determined by X-ray analysis. The complexes were tested as catalysts for the oxidation of cycloalkenes and benzyl alcohol using H O as terminal oxidant. Excellent selectivity was achieved in the oxidation of cyclohexene. © 2013 Springer Science+Business Media Dordrecht.
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=84876467624&origin=inward; http://dx.doi.org/10.1007/s11243-012-9687-z; http://link.springer.com/10.1007/s11243-012-9687-z; http://link.springer.com/content/pdf/10.1007/s11243-012-9687-z; http://link.springer.com/content/pdf/10.1007/s11243-012-9687-z.pdf; http://link.springer.com/article/10.1007/s11243-012-9687-z/fulltext.html; https://dx.doi.org/10.1007/s11243-012-9687-z; https://link.springer.com/article/10.1007%2Fs11243-012-9687-z
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