Development of a comprehensive screening method for more than 300 organic chemicals in water samples using a combination of solid-phase extraction and liquid chromatography-time-of-flight-mass spectrometry
Environmental Science and Pollution Research, ISSN: 1614-7499, Vol: 24, Issue: 34, Page: 26396-26409
2017
- 32Citations
- 55Captures
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Example: if you select the 1-year option for an article published in 2019 and a metric category shows 90%, that means that the article or review is performing better than 90% of the other articles/reviews published in that journal in 2019. If you select the 3-year option for the same article published in 2019 and the metric category shows 90%, that means that the article or review is performing better than 90% of the other articles/reviews published in that journal in 2019, 2018 and 2017.
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Metrics Details
- Citations32
- Citation Indexes32
- 32
- Captures55
- Readers55
- 55
Article Description
A comprehensive screening method for 311 organic compounds with a wide range of physicochemical properties (log Pow −2.2–8.53) in water samples was developed by combining solid-phase extraction with liquid chromatography–high-resolution time-of-flight mass spectrometry. Method optimization using 128 pesticides revealed that tandem extraction with styrene-divinylbenzene polymer and activated carbon solid-phase extraction cartridges at pH 7.0 was optimal. The developed screening method was able to extract 190 model compounds with average recovery of 80.8% and average relative standard deviations (RSD) of 13.5% from spiked reagent water at 0.20 μg L, and 87.1% recovery and 10.8% RSD at 0.05 μg L. Spike-recovery testing (0.20 μg L) using real sewage treatment plant effluents resulted in an average recovery and average RSD of 190 model compounds of 77.4 and 13.1%, respectively. The method was applied to the influent and effluent of five sewage treatment plants in Kitakyushu, Japan, with 29 out of 311 analytes being observed at least once. The results showed that this method can screen for a large number of chemicals with a wide range of physicochemical properties quickly and at low operational cost, something that is difficult to achieve using conventional analytical methods. This method will find utility in target screening of hazardous chemicals with a high risk in environmental waters, and for confirming the safety of water after environmental incidents.
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=85029785850&origin=inward; http://dx.doi.org/10.1007/s11356-017-9929-x; http://www.ncbi.nlm.nih.gov/pubmed/28948438; http://link.springer.com/10.1007/s11356-017-9929-x; https://dx.doi.org/10.1007/s11356-017-9929-x; https://link.springer.com/article/10.1007/s11356-017-9929-x
Springer Nature
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