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PdCl-catalyzed heterocyclotrimerization in MeOH/scCO : A versatile approach to dimethyl pyridine-3,5-dicarboxylate from methyl acrylate and urea

Science in China, Series B: Chemistry, ISSN: 1006-9291, Vol: 51, Issue: 5, Page: 447-451
2008
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Article Description

A novel and green method for the synthesis of dimethyl pyridine-3,5- dicarboxylate has been developed. It is PdCl-catalyzed heterocyclotrimerization of methyl acrylate with urea in methanol/supercritical carbon dioxide. The target compound was obtained with a 75% isolated yield under the optimized conditions. © 2008 Science Press.

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