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An unexpected tetranuclear Li Cr trimethylsilylacetylide complex bridged by two μ -pyrazolates

Science China Chemistry, ISSN: 1674-7291, Vol: 55, Issue: 6, Page: 914-917
2012
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Conference Paper Description

A tetranuclear Li Cr acetylide precursor complex, [Li(Tp)Cr (C CSiMe ) (μ -pz)] •(n-pentane) (Tp = hydridotris(pyrazolyl) borate, pz = pyrazolate) (1) has been synthesized and characterized. The X-ray structure analysis shows that the complex contains a Li Cr core bridged by two μ -pyrazolates. The magnetic data exhibit the existence of weak antiferromagnetic interaction in the cluster. © 2012 Science China Press and Springer-Verlag Berlin Heidelberg.

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