Syntheses, structure and photoluminescent properties of lanthanide oxalatosulfocarboxylate coordination polymers
Chinese Science Bulletin, ISSN: 1001-6538, Vol: 57, Issue: 14, Page: 1659-1664
2012
- 3Citations
- 10Captures
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Article Description
Hydrothermal reactions of oxalic acid (H ox) and 2-sulfobenzoic acid (H L) with lanthanide oxide or hydroxide yielded five lanthanide oxalatosulfocarboxylates. They have a general formula [Ln L (ox)(H O) ] [Ln = La (1), Nd (2), Eu (3), Gd (4), Tb (5)]. Their structures were characterized by single crystal X-ray diffraction, powder X-ray diffraction (PXRD), infrared (IR) spectroscopy, elemental analysis (EA), and thermogravimetric analysis (TGA). 1-5 are isostructural coordination polymers and feature one-dimensional (1D) chains, which are extended into 3D supramolecular frameworks through inter-chain hydrogen bonds between coordinated H O donors and oxygen acceptors from carboxylate, sulfonate and oxalate groups. In addition, the solid-state photoluminescence properties of the Nd (2), Eu (3) and Tb (5) derivatives have been measured at room temperature. The Eu and Tb-containing coordination polymers (CPs) exhibit intense red and green luminescence emissions, respectively, with lifetimes in the order of millisecond. © 2012 The Author(s).
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=84862832277&origin=inward; http://dx.doi.org/10.1007/s11434-012-5049-7; http://link.springer.com/10.1007/s11434-012-5049-7; http://link.springer.com/content/pdf/10.1007/s11434-012-5049-7.pdf; http://link.springer.com/article/10.1007/s11434-012-5049-7/fulltext.html; http://www.springerlink.com/index/10.1007/s11434-012-5049-7; http://www.springerlink.com/index/pdf/10.1007/s11434-012-5049-7; https://dx.doi.org/10.1007/s11434-012-5049-7; https://link.springer.com/article/10.1007/s11434-012-5049-7
Springer Nature
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