Synthesis, characterization, antibacterial activity and VSM investigation of FeO–NiCrO nano oxide obtained from a new oxalato-bridged complex
Chemical Papers, ISSN: 1336-9075, Vol: 72, Issue: 2, Page: 487-495
2018
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- 6Captures
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Article Description
The preparation of FeO–NiCrO nano-oxide (2) is reported via thermal decomposition of [Fe(phen)(HO)][(ox)Cr(μ-ox)Ni(phen)(μ-ox)Cr(ox)] (1) [phen = 1,10-phenanthroline; ox = oxalate] precursor complex for the first time. The complex 1 was characterized by FT-IR spectroscopy and elemental analysis. The thermal stability of complex 1 was also investigated. The composition of the nano oxide 2 was confirmed by energy-dispersive X-ray spectroscopy analysis and the cubic structure, was supported by powder X-ray diffraction. In addition, uniform morphology of the nano-oxide was illustrated by field-emission scanning electron microscopy. The elemental mapping was carried out and presented the distribution of Cr, Fe and Ni ions in nano oxide. In vitro antibacterial activity of 2 was investigated by using IZ and bacterium as per the colony count method against two gram-positive and two gram-negative bacteria. All the experiments revealed that the nano oxide had good effect on deactivating of bacteria. Finally, ferromagnetic behavior of 1 and paramagnetic feature of 2 were measured by vibrating sample magnetometer.
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=85041287439&origin=inward; http://dx.doi.org/10.1007/s11696-017-0301-x; http://link.springer.com/10.1007/s11696-017-0301-x; http://link.springer.com/content/pdf/10.1007/s11696-017-0301-x.pdf; http://link.springer.com/article/10.1007/s11696-017-0301-x/fulltext.html; https://dx.doi.org/10.1007/s11696-017-0301-x; https://link.springer.com/article/10.1007/s11696-017-0301-x
Springer Science and Business Media LLC
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