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Recyclable nickel catalysed Suzuki-Miyaura reaction in the presence of polyethyleneimine under phosphine-free conditions in ethylene glycol

Journal of Chemical Sciences, ISSN: 0973-7103, Vol: 123, Issue: 4, Page: 485-489
2011
  • 4
    Citations
  • 0
    Usage
  • 12
    Captures
  • 0
    Mentions
  • 0
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Metric Options:   Counts1 Year3 Year

Metrics Details

  • Citations
    4
    • Citation Indexes
      4
  • Captures
    12

Article Description

In this report, Suzuki-Miyaura coupling reaction was performed in the presence of polyethyleneimine (PEI) as ligand, NiCl·6H O and KCO in ethylene glycol at 80-100°C under phosphinefree conditions. By this method, structurally different aryl bromides and iodides were reacted with phenylboronic acid and potassium phenyltrifluoroborate. Under these simple reaction conditions a different iaryl derivatives have been prepared in high to excellent yields. Recycling experiments showed that catalyst can be used as recyclable catalyst in the Suzuki-Miyaura cross-coupling reactions. © Indian Academy of Sciences.

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