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Complicated Conformational Exchange of New Pyridoxine Derivative. Dynamic C NMR Characterization

BioNanoScience, ISSN: 2191-1649, Vol: 7, Issue: 4, Page: 555-557
2017
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New pyridoxine derivative with multiple chemical exchanges was studied by C (at 298 K, 188 K) and 2D NMR (H-C HSQC, H-C HMBC) spectroscopy in acetone-d solution. Complete C NMR data (table with chemical shifts at different temperatures) is presented. Intramolecular mobility of the molecule was analyzed based on the results of C NMR experiments in combination with the data obtained from previous study of this compound by dynamic H NMR spectroscopy.

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