Two new palladium and platinum complexes with a bidentate pyrazole-based ligand: Crystal structure, fluorescence and Hirshfeld surface analysis
Journal of the Iranian Chemical Society, ISSN: 1735-2428, Vol: 13, Issue: 5, Page: 823-830
2016
- 6Citations
- 2Captures
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Article Description
Two new precious metal coordination complexes [Pd(HL)] (1) and [PtL] (2) (where HL is 1-(carboxymethyl)-1H-pyrazole-3-carboxylic acid) were synthesized by one-pot in situ hydrolysis. The complexes are assembled into a 3D structure by hydrogen bonding interactions and intermolecular contacts. The structures have been established by single-crystal X-ray diffraction, and characterized by FT-IR and liquid state fluorescent spectroscopy. Hirshfeld surface analysis reveals that the OH contacts outnumber the other contacts in both structures (49.4 % of the total interactions for 1 and 41.6 % for 2).
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=84962231565&origin=inward; http://dx.doi.org/10.1007/s13738-015-0797-3; http://link.springer.com/10.1007/s13738-015-0797-3; http://link.springer.com/content/pdf/10.1007/s13738-015-0797-3; http://link.springer.com/content/pdf/10.1007/s13738-015-0797-3.pdf; http://link.springer.com/article/10.1007/s13738-015-0797-3/fulltext.html; https://dx.doi.org/10.1007/s13738-015-0797-3; https://link.springer.com/article/10.1007/s13738-015-0797-3
Springer Science and Business Media LLC
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