Green synthesis of silver nanoparticles (SNPs)-modified electrode for electrochemical detection of nitrobenzene
Journal of the Iranian Chemical Society, ISSN: 1735-2428, Vol: 17, Issue: 4, Page: 893-900
2020
- 26Citations
- 24Captures
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Article Description
Nitrobenzene (NB) is a highly toxic and hazardous compound that needs to be detected at the low level. The current work describes an eco-friendly synthesis of silver nanoparticles (SNPs) using a Eucalyptus extract as reducing and stabilizing agent and its use for electrochemical detection of NB. The synthesized SNPs were characterized by following techniques UV–visible spectroscopy, powder X-ray diffraction, FESEM, HRTEM and TEM, FTIR spectroscopy. Further electrochemical investigation of SNPs-modified glassy carbon electrode (SNPs/GCE) is carried out by cyclic voltammetric and differential pulse voltammetric techniques. The prepared NPs exhibit excellent electrochemical behaviour towards reduction of NB and show a linear response in the range 5–40 µM, sensitivity of 2.262 µA µM cm and limit of detection of 0.027 µM. SNPs/GCE shows good selectivity towards NB detection. Also, the system exhibits a considerable recovery towards NB detection in of water and waste samples.
Bibliographic Details
http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=85076828593&origin=inward; http://dx.doi.org/10.1007/s13738-019-01822-z; http://link.springer.com/10.1007/s13738-019-01822-z; http://link.springer.com/content/pdf/10.1007/s13738-019-01822-z.pdf; http://link.springer.com/article/10.1007/s13738-019-01822-z/fulltext.html; https://dx.doi.org/10.1007/s13738-019-01822-z; https://link.springer.com/article/10.1007/s13738-019-01822-z
Springer Science and Business Media LLC
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