Synthesis and photooxidation of sodium 1,3-cyclohexadiene-1,4-diethanoate: A new colorless and water-soluble trap of singlet oxygen.
Tetrahedron, ISSN: 0040-4020, Vol: 52, Issue: 6, Page: 2031-2046
1996
- 34Citations
- 18Captures
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Article Description
The sodium 1,3-cyclohexadiene-1,4-diethanoate has been designed as a new colorless trap for the measurement of photogenerated singlet oxygen in aqueous solution. Kinetic studies carried out by flash and steady-state photolysis have shown that this compound interacts with singlet oxygen via a pure chemical quenching with a rate constant k r equal to (2.6 × 10 7 ± 0.3) M −1.s −1. The two products obtained by photooxidation have been identified. The major one (88%) is a stable endoperoxide whereas the minor one (12%) is an hydroperoxide which decomposes into a phenolic derivative by prolongated warming at 37 °C.
Bibliographic Details
http://www.sciencedirect.com/science/article/pii/0040402095010041; http://dx.doi.org/10.1016/0040-4020(95)01004-1; http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=0030046904&origin=inward; https://linkinghub.elsevier.com/retrieve/pii/0040402095010041; http://dx.doi.org/10.1016/0040-4020%2895%2901004-1; https://dx.doi.org/10.1016/0040-4020%2895%2901004-1
Elsevier BV
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