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Methods and Instruments | Scanning Electrochemical Microscopy

Encyclopedia of Electrochemical Power Sources, Page: 105-118
2025
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Book Chapter Description

Scanning electrochemical microscopy is based on the recording of electrolysis currents (Faradaic currents) at a microelectrode (ME) probe that is scanned over the sample. Different working modes are available to couple the electrolysis at the ME to reactions at the sample. The article explains their principles and provides examples of their application. The feedback mode, the sample-generation/tip collection mode, the redox-competition mode and the surface interrogation mode are most frequently applied to the characterization of interphases and interfaces occurring in electrochemical power sources.

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