Synthesis and characterization of neodymium oxyhydroxide crystals
Journal of Alloys and Compounds, ISSN: 0925-8388, Vol: 468, Issue: 1, Page: 566-570
2009
- 12Citations
- 14Captures
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Article Description
Single crystals of neodymium oxyhydroxide NdOOH were grown using an electrochemical method. Crystals having a maximum size of about 2 mm in length were grown. The structure was identified by single crystal X-ray diffraction and the refinement converged to R1 = 0.0170 and wR1 = 0.0426. NdOOH crystallizes in a monoclinic structure of the space group P2 1 / m with lattice parameters of a = 4.3896(2) Å, b = 3.8319(2) Å, c = 6.2424(3) Å, and β = 108.131(2)°, and Z = 2. The resistivity shows semiconductor-like characteristics with the activation energy E a = 0.93 eV. No magnetic order was found down to 5 K.
Bibliographic Details
http://www.sciencedirect.com/science/article/pii/S092583880800114X; http://dx.doi.org/10.1016/j.jallcom.2008.01.056; http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=58049213724&origin=inward; https://linkinghub.elsevier.com/retrieve/pii/S092583880800114X; https://dx.doi.org/10.1016/j.jallcom.2008.01.056
Elsevier BV
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