Spectroelectrochemical study of N -hydroxyphthalimide and phthalimide- N -oxyl generated in an optically transparent thin-layer electrochemical voltammetry
Journal of Electroanalytical Chemistry, ISSN: 1572-6657, Vol: 952, Page: 117956
2024
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Article Description
The combination of a sulfuric acid-acetonitrile mixed electrolyte solution and thin-layer spectroelectrochemical voltammetry enables the measurement of the potential-dependent spectrum of N -hydroxyphthalimide (NHPI) over the visible-ultraviolet-deep-ultraviolet wavelength region. The spectra change reversibly with the application of potential in the potential region where the reversible proton-coupled electron transfer of NHPI occurs. It was found that the absorption band supporting the formation of phthalimide- N -oxyl radical is generated in the deep-ultraviolet region by electro-oxidation.
Bibliographic Details
http://www.sciencedirect.com/science/article/pii/S1572665723008160; http://dx.doi.org/10.1016/j.jelechem.2023.117956; http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=85181722679&origin=inward; https://linkinghub.elsevier.com/retrieve/pii/S1572665723008160; https://dx.doi.org/10.1016/j.jelechem.2023.117956
Elsevier BV
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