High-yield synthesis of alkyl levulinate from furfuryl alcohol and its upgrading to 2-methyl-1,3-dioxolane over AgPW
Molecular Catalysis, ISSN: 2468-8231, Vol: 549, Page: 113477
2023
- 2Citations
- 5Captures
- 1Mentions
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Most Recent News
Studies in the Area of Biofuel Reported from Chinese Academy of Sciences (High-yield Synthesis of Alkyl Levulinate From Furfuryl Alcohol and Its Upgrading To 2-methyl-1,3-dioxolane Over Agpw)
2023 NOV 15 (NewsRx) -- By a News Reporter-Staff News Editor at Energy Daily News -- Research findings on Biotechnology - Biofuel are discussed in
Article Description
In order to relieve greenhouse effect, it is highly urgent to convert carbon-neutral biomass to value-added chemicals and liquid fuels by designing new process. 96.5% yield of biofuel alkyl levulinate was achieved in the alcoholysis of furfuryl alcohol with ethanol over highly active Ag + exchanged H 3 PW 12 O 40 (AgPW) catalyst at low temperature. In situ XRD, 31 P MAS NMR, XPS and NH 3 -TPD results confirm that AgPW contains large amounts of strong acid sites and stable Keggin structure, resulting in the excellent performance. Subsequently, new process was developed to synthesize biofuel 2-methyl-1,3-dioxolanes (MDL) with ∼70% yields via a tandem furfuryl alcohol alcoholysis and acetalization reaction over AgPW. Additionally, MDL can be availably obtained from furfural, xylose and hemicellulose by an integrated multi-step process.
Bibliographic Details
http://www.sciencedirect.com/science/article/pii/S2468823123005606; http://dx.doi.org/10.1016/j.mcat.2023.113477; http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=85168442309&origin=inward; https://linkinghub.elsevier.com/retrieve/pii/S2468823123005606; https://dx.doi.org/10.1016/j.mcat.2023.113477
Elsevier BV
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