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Effect of a stirring process in an isothermal titration microcalorimeter

Thermochimica Acta, ISSN: 0040-6031, Vol: 420, Issue: 1, Page: 163-167
2004
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Article Description

In this paper, it is analysed the way in which the thermodynamic results obtained in an isothermal titration microcalorimeter, with continuous injection of a liquid and a variable mass are affected. Two aspects are presented, the first one refers to a variation in the baseline that takes place when the liquid mass is increased in the laboratory cell, this variation is due to the change in the thermal coupling between the stirrer and its contact with the thermostat. The second aspect is the analysis of the effect of the stirring process and the injection velocity on the homogenization of the remaining mixture in the laboratory cell.

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