Synthesis of [60]fullerene-functionalized rotaxanes
Tetrahedron, ISSN: 0040-4020, Vol: 62, Issue: 9, Page: 1988-1997
2006
- 18Citations
- 16Captures
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Article Description
Synthesis of [60]fullerene (C 60 )-functionalized rotaxanes via Diels–Alder reactions with C 60 is described. Diels–Alder reaction of C 60 and sulfolene moiety as masked diene attached on the wheels of rotaxanes results in high yields of C 60 incorporation. Rotaxanes are prepared by tin-catalyzed urethane-forming end-capping reaction with isocyanate of pseudorotaxane having the wheel carrying C 60 functionality as introduced by the Diels–Alder reaction. The Diels–Alder reaction was accomplished as end-capping reaction between C 60 and pseudorotaxane bearing sultine moiety as masked diene on the axle terminal. A variety of C 60 -containing [2]rotaxanes was prepared in moderate to good yields by these Diels–Alder protocols.
Bibliographic Details
http://www.sciencedirect.com/science/article/pii/S0040402005019290; http://dx.doi.org/10.1016/j.tet.2005.09.149; http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=31944447237&origin=inward; https://linkinghub.elsevier.com/retrieve/pii/S0040402005019290; https://dx.doi.org/10.1016/j.tet.2005.09.149
Elsevier BV
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