Rapid metal-free reduction of aromatic nitro compounds to aromatic amines in MeOH/H 2 O with B 2 pin 2
Tetrahedron, ISSN: 0040-4020, Vol: 162, Page: 134130
2024
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Article Description
The efficient reduction of nitro compounds to their corresponding amino compounds has been a challenging task. In this study, we developed a method for the rapid reduction of aromatic nitro compounds to aromatic amines. The method uses B 2 pin 2 as the reducing agent and NaOH as the base, and the reaction can be completed in 15 min at 50 °C. A range of nitro compounds containing a variety of sensitive functional groups, such as halogen, thioether, cyano, vinyl, and heteroaryl were chemoselectively reduced to the corresponding anilines in good yields.
Bibliographic Details
http://www.sciencedirect.com/science/article/pii/S0040402024003107; http://dx.doi.org/10.1016/j.tet.2024.134130; http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=85197777369&origin=inward; https://linkinghub.elsevier.com/retrieve/pii/S0040402024003107; https://dx.doi.org/10.1016/j.tet.2024.134130
Elsevier BV
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