Synthesis of retro-inverso peptides employing isocyanates of N α -Fmoc-amino acids/peptide acids catalyzed by DMAP
Tetrahedron Letters, ISSN: 0040-4039, Vol: 47, Issue: 51, Page: 9139-9141
2006
- 17Citations
- 9Captures
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Article Description
The Goldschmidt–Wick type reaction between isocyanates of N α -Fmoc-amino acids/peptide acids and N α -Boc-/Z-/Bsmoc-amino acids catalyzed by DMAP leads to the incorporation of a reversed peptide bond. It was found to be a simple, efficient and clean reaction. All the retro-inverso peptides made were obtained as crystalline compounds in 70–92% yields.
Bibliographic Details
http://www.sciencedirect.com/science/article/pii/S0040403906020831; http://dx.doi.org/10.1016/j.tetlet.2006.10.066; http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=33751107195&origin=inward; https://linkinghub.elsevier.com/retrieve/pii/S0040403906020831; https://dx.doi.org/10.1016/j.tetlet.2006.10.066
Elsevier BV
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