Tandem Pd-catalyzed C–C coupling/recyclization of 2-(2-bromoaryl)cyclopropane-1,1-dicarboxylates with primary nitro alkanes
Tetrahedron Letters, ISSN: 0040-4039, Vol: 57, Issue: 1, Page: 11-14
2016
- 23Citations
- 23Captures
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Article Description
The first successful synthesis of 1 H -2,3-benzoxazine 3-oxides has been described. The efficiency of the approach is provided by the C–C-coupling of 2-(2-bromoaryl)cyclopropane-1,1-dicarboxylates with primary nitroalkanes catalyzed by Pd(dba) 2 /JohnPhos system followed by in situ recyclization of the intermediates. Several representative transformations allowing selective modification of the nitronate as well as malonate functionalities in the resulting compounds are demonstrated.
Bibliographic Details
http://www.sciencedirect.com/science/article/pii/S0040403915302884; http://dx.doi.org/10.1016/j.tetlet.2015.10.091; http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=84949921007&origin=inward; https://linkinghub.elsevier.com/retrieve/pii/S0040403915302884; https://dx.doi.org/10.1016/j.tetlet.2015.10.091
Elsevier BV
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