Direct conversion of sec -phosphine oxides to sec -phosphine-boranes using BH 3
Tetrahedron Letters, ISSN: 0040-4039, Vol: 67, Page: 152837
2021
- 5Citations
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Article Description
An effective and mild synthetic method for secondary phosphine-boranes from secondary phosphine oxides was developed. The slow addition of borane-tetrahydrofuran to a solution of secondary phosphine oxides at ambient temperature gave secondary phosphine-boranes with high yield. The use of air-sensitive secondary phosphines, which are common substrates for secondary phosphine-borane syntheses, is avoided in this mild process. Moreover, generation of by-products, such as secondary hydroxy-phosphine-boranes, is also minimized.
Bibliographic Details
http://www.sciencedirect.com/science/article/pii/S0040403921000174; http://dx.doi.org/10.1016/j.tetlet.2021.152837; http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=85101303877&origin=inward; https://linkinghub.elsevier.com/retrieve/pii/S0040403921000174; https://api.elsevier.com/content/article/PII:S0040403921000174?httpAccept=text/xml; https://api.elsevier.com/content/article/PII:S0040403921000174?httpAccept=text/plain; https://dul.usage.elsevier.com/doi/; https://dx.doi.org/10.1016/j.tetlet.2021.152837
Elsevier BV
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