The ultrasound-assisted oxidative scission of monoenic fatty acids by ruthenium tetroxide catalysis: Influence of the mixture of solvents
Ultrasonics Sonochemistry, ISSN: 1350-4177, Vol: 16, Issue: 2, Page: 266-272
2009
- 35Citations
- 23Captures
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Example: if you select the 1-year option for an article published in 2019 and a metric category shows 90%, that means that the article or review is performing better than 90% of the other articles/reviews published in that journal in 2019. If you select the 3-year option for the same article published in 2019 and the metric category shows 90%, that means that the article or review is performing better than 90% of the other articles/reviews published in that journal in 2019, 2018 and 2017.
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Metrics Details
- Citations35
- Citation Indexes35
- CrossRef35
- 31
- Captures23
- Readers23
- 23
Article Description
Carboxylic acids and diacids were synthesized from monoenic fatty acids by using RuO 4 catalysis, under ultrasonic irradiation, in various mixtures of solvents. Ultrasound associated with Aliquat ® 336 have promoted in water, the quantitative oxidative cleavage of the CH CH bond of oleic acid. A design of experiment (DOE) shows that the optimal mixture of solvents (H 2 O/MeCN, ratio 1/1, 2.2% RuCl 3 /4.1 eq. NaIO 4 ) gives 81% azelaic acid and 97% pelargonic acid. With the binary heterogeneous mixture H 2 O/AcOEt, the oxidation of the oleic acid leads to a third product, the α-dione 9,10-dioxostearic acid.
Bibliographic Details
http://www.sciencedirect.com/science/article/pii/S1350417708001302; http://dx.doi.org/10.1016/j.ultsonch.2008.08.003; http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=54349091494&origin=inward; http://www.ncbi.nlm.nih.gov/pubmed/18799341; https://linkinghub.elsevier.com/retrieve/pii/S1350417708001302; https://dx.doi.org/10.1016/j.ultsonch.2008.08.003
Elsevier BV
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