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Ultrasonic irradiation assisted syntheses of one-dimensional di(azido)-dipyridylamine Cu(II) coordination polymer nanoparticles

Ultrasonics Sonochemistry, ISSN: 1350-4177, Vol: 23, Page: 208-211
2015
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Article Description

The Cu(II) coordination polymer, [Cu(dpa)(N 3 ) 2 ] n ( 1 ), has been synthesized by the reaction of 2,2′-dipyridylamine (dpa) and a mixture of Cu(ClO 4 ) 2 ·6H 2 O and sodium azide under ultrasonic irradiation. The products were characterized by infrared (FT-IR) spectroscopy, X-ray powder diffraction, and scanning electron microscopy (SEM). The CuO nano particles were prepared from calcination of compound 1 at 873 K. The CuO nanoparticles were characterized by X-ray powder diffraction (XRD), scanning electron microscopy (SEM). This study demonstrates that sonochemistry is a suitable method for the preparation of coordination polymer nano-structures and that the calcination temperature can be an effective parameter to control the size of CuO nano-structures prepared by direct calcination of a coordination polymer.

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