Rheological measurements in titania gels synthesized from reverse micelles
Chemical Physics Letters, ISSN: 0009-2614, Vol: 323, Issue: 1, Page: 93-97
2000
- 21Citations
- 5Captures
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Article Description
TiO 2 sol and gel systems have been synthesized by hydrolysis of titanium butoxide in microemulsions W/O. Different systems compositions were prepared at constant W o =[H 2 O]/[AOT] and changing R =[H 2 O]/[Ti(BuO) 4 ]. Experimental measurements show a progressive increase of the viscosity with time, characteristic of a sol–gel transition. The rheology of the transition was studied by following the behavior of viscoelastic parameters ( G ′, G ″ and η *) as a function of time at different frequencies. The possibility to apply standard percolation theory was discussed. The application of two alternative growth models — either `fractal growth model' or `nearly linear growth model' — has been analysed.
Bibliographic Details
http://www.sciencedirect.com/science/article/pii/S000926140000498X; http://dx.doi.org/10.1016/s0009-2614(00)00498-x; http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=0037572934&origin=inward; http://linkinghub.elsevier.com/retrieve/pii/S000926140000498X; http://api.elsevier.com/content/article/PII:S000926140000498X?httpAccept=text/xml; http://api.elsevier.com/content/article/PII:S000926140000498X?httpAccept=text/plain; https://linkinghub.elsevier.com/retrieve/pii/S000926140000498X; https://dul.usage.elsevier.com/doi/; https://api.elsevier.com/content/article/PII:S000926140000498X?httpAccept=text/xml; https://api.elsevier.com/content/article/PII:S000926140000498X?httpAccept=text/plain; http://dx.doi.org/10.1016/s0009-2614%2800%2900498-x; https://dx.doi.org/10.1016/s0009-2614%2800%2900498-x
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