31 P NMR study of magnesium phosphate glasses
Journal of Non-Crystalline Solids, ISSN: 0022-3093, Vol: 283, Issue: 1, Page: 88-94
2001
- 62Citations
- 49Captures
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Article Description
1-D magic angle spinning (MAS) and 2-D double quantum solid-state 31P nuclear magnetic resonance (NMR) investigations have been carried out on (MgO) x (P 2 O 5 ) 1−x glasses over compositional range from x =0.44 to 0.59. The distribution of the Q n phosphate units, obtained from the simulation of 31P MAS spectra, is close to a binary distribution of bridging and non-bridging oxygen atoms, indicating that the Mg 2+ cations act as network modifiers. High-resolution 31P double quantum NMR is used to probe the intermediate range order in phosphate glasses and suggests that the anomalous behavior near the metaphosphate composition is due to a change from ring structures to phosphate chains.
Bibliographic Details
http://www.sciencedirect.com/science/article/pii/S002230930100357X; http://dx.doi.org/10.1016/s0022-3093(01)00357-x; http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=0035340012&origin=inward; https://linkinghub.elsevier.com/retrieve/pii/S002230930100357X; https://api.elsevier.com/content/article/PII:S002230930100357X?httpAccept=text/xml; https://api.elsevier.com/content/article/PII:S002230930100357X?httpAccept=text/plain; http://linkinghub.elsevier.com/retrieve/pii/S002230930100357X; http://api.elsevier.com/content/article/PII:S002230930100357X?httpAccept=text/xml; http://api.elsevier.com/content/article/PII:S002230930100357X?httpAccept=text/plain; http://dx.doi.org/10.1016/s0022-3093%2801%2900357-x; https://dx.doi.org/10.1016/s0022-3093%2801%2900357-x
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