Formation and characterization of Al 10 CaFe 2 compound in Al−Ca−Fe alloys
Transactions of Nonferrous Metals Society of China, ISSN: 1003-6326, Vol: 34, Issue: 2, Page: 361-377
2024
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Article Description
The phase diagram of the Al−Ca−Fe system in the aluminum corner, including the liquidus projection and solidification reactions, was studied by using thermodynamic calculations and experimental techniques. The results show that instead of the Al 3 Fe phase, a ternary compound whose composition corresponds to the formula Al 10 CaFe 2 should be in equilibrium with the aluminum solid solution (Al). Thе transition from the binary to the ternary compound occurs via the peritectic transformation L + Al 3 Fe → (Al) + Al 10 CaFe 2 (at 638 °C, 3.3 at.% Ca and 0.5 at.% Fe). Primary and eutectic crystals of the ternary compound have a compact morphology, in contrast to needle-shaped inclusions of the Al 3 Fe phase. First principles calculations and X-ray diffraction analysis were used to determine the crystal lattice structure of Al 10 CaFe 2 ternary compound. In addition, the near eutectic alloy Al−6wt.%Ca−1wt.%Fe after annealing at 500−600 °C has a fine structure with a total fraction of excess phases of about 25 vol.%. Thus, the Al−Ca−Fe system can be used to create new aluminum-matrix composite alloys.
Bibliographic Details
http://www.sciencedirect.com/science/article/pii/S1003632623664040; http://dx.doi.org/10.1016/s1003-6326(23)66404-0; http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=85189855756&origin=inward; https://linkinghub.elsevier.com/retrieve/pii/S1003632623664040; http://dx.doi.org/10.1016/s1003-6326%2823%2966404-0; https://dx.doi.org/10.1016/s1003-6326%2823%2966404-0; http://sciencechina.cn/gw.jsp?action=cited_outline.jsp&type=1&id=7738259&internal_id=7738259&from=elsevier
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