Crystal growth of Ag M OF (M = V, x = 2; M = Mo, x = 3)
Crystal Growth and Design, ISSN: 1528-7483, Vol: 10, Issue: 11, Page: 4868-4873
2010
- 31Citations
- 12Captures
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Conference Paper Description
Understanding the complex relationship between synthesis conditions, in particular temperature and composition, led to single crystals of the cryolite type phases AgMoOF and AgVO F. These crystals form in a reversible thermodynamic process from dissolved species when the solution is heated. Single crystal structural data reveal the Mo cation distorted toward facially coordinated oxides for AgMoOF, and the V cation toward the edge of the cis-oxide positions for Ag VOF. Local ordering of oxide and fluoride ligands is observed for both structures. © 2010 American Chemical Society.
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