Transformation of organosilicon-loaded alumina gel to homogeneous alumino-silicates: A solid-state NMR study
Chemistry of Materials, ISSN: 0897-4756, Vol: 13, Issue: 2, Page: 247-249
2001
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Article Description
A novel approach for the preparation of homogeneous bicomponent oxides, which does not require a cogelation process, is presented. Homogeneous Si/Al oxides were obtained by heating in air alumina gels with physically entrapped (MeSi)Si or (ClMeSi)Si, which were dispersed inside the alumina gel during the nonhydrolytic condensation of AlCl with PrO. The formation of Si-O-Al linkages upon heating and the homogeneity of the Si/Al oxides were evidenced by Si and Al solid-state NMR spectroscopy.
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