Structure and properties of [CrF(NCMe)](BF )·MeCN: A nonaqueous source of Cr F and a building block for new Prussian-blue-like magnetic materials
Inorganic Chemistry, ISSN: 0020-1669, Vol: 47, Issue: 17, Page: 7768-7774
2008
- 14Citations
- 21Captures
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Metrics Details
- Citations14
- Citation Indexes14
- CrossRef14
- 13
- Captures21
- Readers21
- 21
Article Description
[CrF(NCMe)](BF)· MeCN (1) was synthesized from a prolonged dissolution of [Cr(NCMe) ](BF) in MeCN via fluoride abstraction from BF. Complex 1 exhibits a crystal field splitting, Δ, of 17 470 cm and is a nonaqueous source of CrF. The reaction of 1 with (NEt) [Cr(CN)] formed a new Prussian-blue-like magnetic material of (NEt)[CrF] [Cr(CN)](BF) ·0.10(MeCN) (2) composition. Complex 2 magnetically orders at a critical temperature, T, of 85 K and at 2 K exhibits magnetic hysteresis with a coercive field, H, of 60 Oe and a remanent magnetization, M, of 1880 emuOe/mol. © 2008 American Chemical Society.
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