Synthesis of 1-borylisoindoles via palladium-catalyzed dehydrogenation/C-H borylation of isoindolines
Journal of the American Chemical Society, ISSN: 0002-7863, Vol: 131, Issue: 17, Page: 6070-6071
2009
- 58Citations
- 41Captures
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Metrics Details
- Citations58
- Citation Indexes58
- CrossRef58
- 57
- Captures41
- Readers41
- 41
Article Description
1-Boryl- and 1,3-diborylisoindoles were synthesized by the palladium-catalyzed reaction of isoindolines with pinacolborane via sequential dehydrogenation and C-H borylation. Selective formation of the borylated isoindoles was achieved using Pd(dba)/MeS as the catalyst, in which MeS suppressed the formation of 1-boryl-4,5,6,7-tetrahydroisoindoles. Diborylisoindole was crosscoupled with iodobenzene, giving 1,3-diphenylisoindole in high yield. © 2009 American Chemical Society.
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