A highly efficient microwave-assisted Suzuki coupling reaction of aryl perfluorooctylsulfonates with boronic acids
Organic Letters, ISSN: 1523-7060, Vol: 6, Issue: 9, Page: 1473-1476
2004
- 104Citations
- 35Captures
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Metrics Details
- Citations104
- Citation Indexes104
- 104
- CrossRef93
- Captures35
- Readers35
- 35
Article Description
A new strategy to improve the efficiency of Suzuki coupling reactions is introduced by combining fast microwave reaction with easy fluorous separation. Aryl perfluorooctylsulfonates derived from the corresponding phenols are coupled with aryl boronic acids to form biaryls under general microwave conditions. Both intermediates and products are purified by solid-phase extraction over Fluoro Flash silica gel. Application of this tagging strategy to multistep synthesis of biaryl-substituted hydantoin is also described.
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